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CAS No. : | 226085-17-2 | MDL No. : | MFCD08689737 |
Formula : | C12H13BrN2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 297.15 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338-P310 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
79% | at -20 - 20℃; for 2 h; | To a solution of 3-bromo-1-H-pyrrolo[2,3-b]pyridine (0.10 g, 0.50 mmol) in THF (4.0 mL) under nitrogen atmosphere was added DMAP (0.006 g, 0.06 mmol). The resulting reaction mixture was cooled to -2O0C followed by addition of Boc anhydride (122 μL, 0.56 mmol). The reaction mixture ws then allowed to warm upto room temperature and stirred for 2 h. After the completion of reaction (TLC monitoring), water (20 mL) was added to the reaction mixture and then extracted with EtOAc (3 x 50 mL). The combined organics was dried (Na2SO4), filtered and concentrated. The residue was purified over silica gel (60-120 M, 5percent EtOAc-Hexane) to obtain the desired product as oily mass (0.12 g, 79percent). |
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