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Chemical Structure| 23092-23-1 Chemical Structure| 23092-23-1

Structure of 23092-23-1

Chemical Structure| 23092-23-1

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Product Details of [ 23092-23-1 ]

CAS No. :23092-23-1
Formula : C11H14O
M.W : 162.23
SMILES Code : C=C(C)CC(C1=CC=CC=C1)O

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Application In Synthesis of [ 23092-23-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23092-23-1 ]

[ 23092-23-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 40263-57-8 ]
  • [ 23092-23-1 ]
  • 2-iodo-3-((3-methyl-1-phenylbut-3-en-1-yl)oxy)pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
30% With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20℃; for 12h;Inert atmosphere; General procedure: The alcohol (1 equiv), phenol (1 equiv) and PPh3 (1.1 equiv) were added to a flask and was purged h argon for 10 minutes. The contents were then dissolved in anhydrous THF (0.66 M) and the resultant solution was cooled to 0 C. At this time, DIAD (1.1 equiv) was added dropwise and then the reaction mixture was warmed to room temperature for 12 hours. After the indicated time, the reaction was quenched with H2O and extracted with EtOAc (3x). The combined organic layers were washed with brine, dried over Na2SO4 and concentrated in vacuo. The pure aryl ether was purified via Si gel flash chromatography using the indicated mobile phase.
 

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