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Chemical Structure| 24056-34-6 Chemical Structure| 24056-34-6

Structure of 24056-34-6

Chemical Structure| 24056-34-6

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Product Details of [ 24056-34-6 ]

CAS No. :24056-34-6
Formula : C7H11NO
M.W : 125.17
SMILES Code : OC1CCC(CC1)C#N
MDL No. :MFCD13688990
InChI Key :WXWQWXGBEHIOBL-UHFFFAOYSA-N
Pubchem ID :12617272

Safety of [ 24056-34-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 24056-34-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 24056-34-6 ]

[ 24056-34-6 ] Synthesis Path-Upstream   1~4

  • 1
  • [ 34916-10-4 ]
  • [ 24056-34-6 ]
YieldReaction ConditionsOperation in experiment
99% at 0 - 20℃; for 1 h; Inert atmosphere Into a 250-mL 4-necked round-bottom flask purged and maintained with an inert atmosphere of nitrogen, was placed 119.1 (10 g, 81.20 mmol, 1.00 equiv), methanol (100 mL). This was followed by the addition of NaBH4 (1.52 g, 40.18 mmol, 0.50 equiv) at 0° C. in a water/ice bath. The resulting solution was stirred for 1 h at room temperature. The reaction was then quenched by the addition of 20 mL of NH4Cl (aq). The resulting solution was extracted with 2×100 mL of ethyl acetate and the organic layers combined and dried over anhydrous sodium sulfate and concentrated under vacuum. This resulted in 10.02 g (99percent) of 119.2 as colorless oil.
References: [1] Patent: US2017/166584, 2017, A1, . Location in patent: Paragraph 0887-0889.
[2] Annales de Chimie (Cachan, France), 1955, vol. <12> 10, p. 497,531.
[3] Bulletin de la Societe Chimique de France, 1954, p. 610,612.
[4] Patent: WO2009/156100, 2009, A1, . Location in patent: Page/Page column 156.
  • 2
  • [ 766-05-2 ]
  • [ 24056-33-5 ]
  • [ 196801-10-2 ]
  • [ 24056-34-6 ]
  • [ 108-94-1 ]
References: [1] Angewandte Chemie - International Edition, 2014, vol. 53, # 33, p. 8659 - 8663.
  • 3
  • [ 69947-09-7 ]
  • [ 24056-34-6 ]
References: [1] Patent: WO2009/156100, 2009, A1, .
  • 4
  • [ 13482-22-9 ]
  • [ 38622-91-2 ]
  • [ 24056-34-6 ]
References: [1] Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1980, vol. 35, # 11, p. 1451 - 1454.
 

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