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Chemical Structure| 24070-16-4 Chemical Structure| 24070-16-4

Structure of 24070-16-4

Chemical Structure| 24070-16-4

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Product Details of [ 24070-16-4 ]

CAS No. :24070-16-4
Formula : C21H21NO
M.W : 303.40
SMILES Code : OCCNC(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3
MDL No. :MFCD00399829

Safety of [ 24070-16-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 24070-16-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24070-16-4 ]

[ 24070-16-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2002-24-6 ]
  • [ 76-83-5 ]
  • [ 121-44-8 ]
  • [ 75-05-8 ]
  • [ 24070-16-4 ]
YieldReaction ConditionsOperation in experiment
In dichloromethane; Step A N-tritylethanolamine Ethanolamine hydrochloride (9.9 g; 100 mmol) is partially dissolved in CH2 Cl2 /CH3 CN (200 ml/100 ml) and Et3 N (23 ml; 170 mmol) is then added. Tritylchloride (18.9 g; 67.6 mmol) is added portionwise over 30 minutes. After the addition is complete the reaction mixture is allowed to stir an additional 30 minutes, diluted with CH2 Cl2, washed With H2 O 2* and brine, dried (MgSO4), concentrated in vacuo and purified by column chromatography with silica/CH2 Cl2 to give N-tritylethanolamine as an oil which is used directly in Step B.
 

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