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Chemical Structure| 243984-26-1 Chemical Structure| 243984-26-1

Structure of 243984-26-1

Chemical Structure| 243984-26-1

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Product Details of [ 243984-26-1 ]

CAS No. :243984-26-1
Formula : C9H13ClO4S
M.W : 252.72
SMILES Code : O=C(C1=C(S(=O)(Cl)=O)CCCC1)OCC
MDL No. :MFCD16038956

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Application In Synthesis of [ 243984-26-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 243984-26-1 ]

[ 243984-26-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 243984-26-1 ]
  • [ 367-34-0 ]
  • ethyl 6-[N-(2,4,5-trifluorophenyl)sulfamoyl]-1-cyclohexene-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Example 40 By the procedure similar to that employed in Example 33, ethyl 2-chlorosulfonyl-1-cyclohexene-1-carboxylate (0.40 g) obtained in Reference Example 2 was reacted with <strong>[367-34-0]2,4,5-trifluoroaniline</strong> (0.31 g) to yield ethyl 6-[N-(2,4,5-trifluorophenyl)sulfamoyl]-1-cyclohexene-1-carboxylate (Compound 43; 0.30 g) as white crystals. 1H-NMR (d6-DMSO)delta: 1.13 (3H, t, J=7.0 Hz), 1.55-1.85 (2H, m), 1.96-2.48 (4H, m), 4.05 (2H, q, J=7.0 Hz), 4.35 (1H, d, J=4.4 Hz), 7.14 (1H, br), 7.47-7.71 (2H, m), 10.17 (1H, s).
 

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