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Chemical Structure| 244-78-0 Chemical Structure| 244-78-0

Structure of 244-78-0

Chemical Structure| 244-78-0

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Product Details of [ 244-78-0 ]

CAS No. :244-78-0
Formula : C10H7N3
M.W : 169.18
SMILES Code : C1(C2=C3C=CN=C2)=C(N3)C=CN=C1

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Application In Synthesis of [ 244-78-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 244-78-0 ]

[ 244-78-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 24686-78-0 ]
  • [ 244-78-0 ]
  • 2
  • [ 2050-48-8 ]
  • [ 244-78-0 ]
  • C32H20N6O2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; copper(l) iodide; 18-crown-6 ether; potassium carbonate; at 180℃; for 48h;Inert atmosphere; Add compound 17 (2 g, 5.3 mmol), compound 42 (2.08 g, 10.6 mmol), cuprous iodide (0.1 g, 0.53 mmol) in a 25 ml single-necked flask.K2CO3 (1.30 g, 13.25 mmol) and 18-crown-6 (0.14 g, 0.53 mmol) were dissolved in 10 mL of MPU solution. Under the protection of N2, the temperature was raised to 180 C and the reaction was carried out for 48 h.After the reaction was terminated, it was cooled to room temperature, extracted, and dried, dichloromethane: methanol 15:1 over column, yield: 60%.
 

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