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[ CAS No. 245-37-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 245-37-4
Chemical Structure| 245-37-4
Structure of 245-37-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 245-37-4 ]

CAS No. :245-37-4 MDL No. :MFCD18836968
Formula : C11H8N2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 168.19 Pubchem ID :-
Synonyms :

Safety of [ 245-37-4 ]

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Application In Synthesis of [ 245-37-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 245-37-4 ]

[ 245-37-4 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 245-37-4 ]
  • [ 5779-94-2 ]
  • [ 272458-07-8 ]
YieldReaction ConditionsOperation in experiment
95% With potassium hydroxide In benzyl alcohol at 40℃; for 48h;
  • 2
  • [iridium(III)(μ-chloro)(2-phenylpyridine)2]2 [ No CAS ]
  • [ 245-37-4 ]
  • [ 2386-53-0 ]
  • [ 1361061-34-8 ]
  • 3
  • [ 245-37-4 ]
  • [ 578743-87-0 ]
  • [(4,5-diazafluorenide)Cu(N,N′-bis(2,6-diisopropylphenyl)-imidazol-2-ylidene)] [ No CAS ]
  • 4
  • [ 245-37-4 ]
  • [ 65610-14-2 ]
  • C27H12N6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 18-crown-6 ether; potassium carbonate In N,N-dimethyl-formamide; toluene at 140℃; for 10h; 1-1 4,5-diazofluorene(20 mmol),4-fluorophthalonitrile (22 mmol),18 crown 6 ether (5.15 mmol) and potassium carbonate (24 mmol) were added to a 25 mL three-necked flask,Further, 10 mL of N, N-dimethylformamide and 3 ml of toluene were added,Heated to 140 ° C, reacted for 10 h,The reaction solution was poured into a large amount of ice water, allowed to stand for precipitation, filtered and washed with water to obtain a crude product.The resulting crude product was dissolved in acetonitrile and the resulting solution was filtered,The filtrate is mixed with a large amount of distilled water and allowed to stand,Precipitation of yellow solid,Filtered and washed with water,To give a compound of formula I.
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