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CAS No. : | 2461-40-7 | MDL No. : | MFCD05865249 |
Formula : | C7H12O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | YLNSNVGRSIOCEU-UHFFFAOYSA-N |
M.W : | 144.17 | Pubchem ID : | 137606 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P501-P261-P270-P202-P210-P201-P271-P264-P280-P370+P378-P308+P313-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330-P302+P352+P312-P304+P340+P312-P403+P235-P405 | UN#: | N/A |
Hazard Statements: | H302+H312+H332-H315-H319-H341-H227 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
> 99 % ee | With thermomyces lanuginosa In 1,4-dioxane; aq. phosphate buffer at 30℃; for 2 h; Resolution of racemate; Enzymatic reaction | General procedure: In a 50 mL erlenmeyer flask containing 6 mL of phosphate buffer (1 M, pH 7), it was added the ester (0.36 mmol), lipase (5 mg), and dioxane (0.6 mL). The mixture was shaken (150 rpm) at 30 °C or 50 °C for a specified period of time (Table 2), while the pH was maintained at 7 by the periodic addition of aqueous 1 M solution of NaOH. It was considered 50percent hydrolysis of the substrate when half the equimolar amount of NaOH was consumed and, an aliquot of the reaction mixture was taken and analyzed by chiral HPLC or GC. |