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Chemical Structure| 24622-15-9 Chemical Structure| 24622-15-9

Structure of 24622-15-9

Chemical Structure| 24622-15-9

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Product Details of [ 24622-15-9 ]

CAS No. :24622-15-9
Formula : C4Cl4O2S2
M.W : 285.98
SMILES Code : O=S(C1=C(Cl)C(Cl)=C(Cl)S1)(Cl)=O
MDL No. :MFCD26395198

Safety of [ 24622-15-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H311-H314-H331
Precautionary Statements:P260-P264-P270-P271-P280-P301+P330+P331-P302+P352-P303+P361+P353-P304+P340-P305+P351+P338-P310-P403+P233-P405-P501
Class:8(6.1)
UN#:2923
Packing Group:

Application In Synthesis of [ 24622-15-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24622-15-9 ]

[ 24622-15-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 24622-15-9 ]
  • [ 4774-10-1 ]
  • [ 809239-73-4 ]
YieldReaction ConditionsOperation in experiment
With potassium tert-butylate; In tetrahydrofuran; at 0 - 20℃; for 2h; A solution of <strong>[4774-10-1]3-methoxypyrazin-2-amine</strong> (3.5 g) and the product from step (a) (8.0g) in drytetrahydrofuran (35 ml) was treated with potassium f-butoxide (1 M solution intetrahydrofuran, 62 ml), dropwise at 0C, under a nitrogen atmosphere. The brownsuspension was allowed to warm to room temperature over 2 hours and was then pouredinto 2 M hydrochloric acid and extracted into ethyl acetate. The combined organic extractswere purified on a pad of flash silica which was eluted with ethyl acetate. Concentrationof the solvent afforded the titled compound as a brown powder (8.4 g). m/e 374/376 (M-l)', 100percent.JH NMR (D6-DMSO) 5 7.79 (1H, br), 7.69 (1H, br), 3.92 (3H, s).MP 212-214C.Elemental Analysis:Theory: C 28.85, H 1.61, N 11.22 percentFound: C 28.72, H 1.88, N 11.23 percent
 

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