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Chemical Structure| 24909-68-0 Chemical Structure| 24909-68-0

Structure of 24909-68-0

Chemical Structure| 24909-68-0

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Product Details of [ 24909-68-0 ]

CAS No. :24909-68-0
Formula : C36H62O3
M.W : 542.88
SMILES Code : CCCCC/C=C\C/C=C\CCCCCCCC(OC(CCCCCCC/C=C\C/C=C\CCCCC)=O)=O
MDL No. :MFCD00010456

Safety of [ 24909-68-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 24909-68-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24909-68-0 ]

[ 24909-68-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 24909-68-0 ]
  • [ 2934-05-6 ]
  • [ 1338939-12-0 ]
YieldReaction ConditionsOperation in experiment
84% With dmap; In dichloromethane; for 10h;Darkness; General procedure: Synthesis of the compounds was accomplished using method of Siddiqui et al. [10] with some modifications. Firstly, 1 mmol of a respective PUFA was dissolved in 5 ml dichloromethane (DCM). Subsequently, 0.45 mmol of coupling reagent N,N-dicyclohexylcarbodiimide (DCC) was added and the reaction mixture was stirred for 10 min at room temperature (23-25 C). Finally, 1 mmol of one of the propofol isomer (2,6-propofol/2,4-propofol) was dissolved and reaction mixture was esterified in the presence of a catalyst, 0.152 mmol 4-dimethylaminopyridine (DMAP). The reaction mixture was stirred for a period of 10 h in dark. Reaction was stopped by filtration and the filtrate was concentrated under reduced pressure to get the product. The progression of reaction and synthesis of product was visualized by thin layer chromatography (TLC) followed by exposure to iodine vapour. Finally, the synthesized compound was purified by silica gel column chromatography with solvent system n-hexane and diethyl ether (1:1).
 

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