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CAS No. : | 25016-01-7 | MDL No. : | MFCD00003347 |
Formula : | C8H7BrO2 | Boiling Point : | 289.1°C at 760 mmHg |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 215.04 g/mol | Pubchem ID : | 90684 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
97% | for 15 h; Reflux | 5-Bromo-2-methoxybenzaldehyde (20.00 mmol, 4.30 g) was dissolved in formic acid (20 mL) and treated with hydroxylamine hydrochloride (21.00 mmol, 1.45 g) and sodium acetate (26.00 mmol, 2.13 g). The reaction mixture was heated at reflux for 15 hours. The solvent was removed under reduced pressure and the residue was taken up in ethyl acetate (250 mL). The organics were washed with saturated sodium bicarbonate solution (2.x.200 mL) and then dried with MgSO4. The organics were filtered and evaporated under reduced pressure to yield the title compound as a white solid. Yield=4.10 g, 97percent. Analytical LCMS method 2, retention time 6.07 min, M+H=214, 216. 1H NMR: (CDCl3) δ: 7.66-7.61 (m, 2H), 6.87 (d, 1H), 3.92 (s, 3H). |
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