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[ CAS No. 2549-53-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
3d Animation Molecule Structure of 2549-53-3
Chemical Structure| 2549-53-3
Chemical Structure| 2549-53-3
Structure of 2549-53-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 2549-53-3 ]

CAS No. :2549-53-3 MDL No. :MFCD00085280
Formula : C18H34O2 Boiling Point : -
Linear Structure Formula :- InChI Key :ATZHWSYYKQKSSY-UHFFFAOYSA-N
M.W : 282.46 Pubchem ID :17351
Synonyms :

Safety of [ 2549-53-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 2549-53-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2549-53-3 ]

[ 2549-53-3 ] Synthesis Path-Downstream   1~4

YieldReaction ConditionsOperation in experiment
vinyl caprinate, particularly vinyl laurate vinyl myristate, as well as C8-14 alkyl (meth)acrylates, such as ... octyl methacrylate nonyl methacrylate decyl methacrylate lauryl methacrylate myristyl methacrylate.
  • 4
  • [ 79-41-4 ]
  • [ 112-72-1 ]
  • [ 2549-53-3 ]
YieldReaction ConditionsOperation in experiment
With toluene-4-sulfonic acid; hydroquinone; In toluene; at 60.0℃;Reflux; 2) In a 500 mL four-necked flask equipped with a thermocouple, a stirrer, a water separator, and a reflux condenser,Add an appropriate amount of tetradecanol, toluene (solvent), hydroquinone (polymerization inhibitor), and p-toluenesulfonic acid (catalyst), and heat them to 60C to completely dissolve them.Then add a methacrylic acid so that the molar ratio of methacrylic acid and tetradecanol is 1:1, the amount of toluene is 75% of the total mass of methacrylic acid and tetradecanol, and the amount of hydroquinone is methacrylic acid and The total mass of tetradecanol is 0.5%, and the amount of p-toluenesulfonic acid is 1.0% of the total mass of methacrylic acid and tetradecanol; 3) continue to heat up to the reflux temperature, the water generated by the reaction carried by the water-bearing agent toluene, in the water separator layer;4) When the reaction reaches the theoretical amount of water, the reaction is completed, the reaction is stopped, excess methacrylic acid and toluene are distilled off under reduced pressure, washed with a mass fraction of 5% alkalinity until the lower aqueous layer is colorless, and then saturated NaCl is used. The solution was washed to neutrality and the pH was 7;5) Take an appropriate amount of anhydrous calcium chloride to dry the product, suction filtration, and vacuum drying in a vacuum oven for more than 48 hours to obtain pure tetradecyl methacrylate.
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