Alternatived Products of [ 2549-53-3 ]
Product Details of [ 2549-53-3 ]
CAS No. : | 2549-53-3 |
MDL No. : | MFCD00085280 |
Formula : |
C18H34O2
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | ATZHWSYYKQKSSY-UHFFFAOYSA-N |
M.W : |
282.46
|
Pubchem ID : | 17351 |
Synonyms : |
|
Application In Synthesis of [ 2549-53-3 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 2549-53-3 ]
- 1
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[ 112-72-1 ]
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[ 760-93-0 ]
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[ 2549-53-3 ]
Yield | Reaction Conditions | Operation in experiment |
|
|
vinyl caprinate, particularly vinyl laurate vinyl myristate, as well as C8-14 alkyl (meth)acrylates, such as ... octyl methacrylate nonyl methacrylate decyl methacrylate lauryl methacrylate myristyl methacrylate. |
- 4
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[ 79-41-4 ]
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[ 112-72-1 ]
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[ 2549-53-3 ]
Yield | Reaction Conditions | Operation in experiment |
|
With toluene-4-sulfonic acid; hydroquinone; In toluene; at 60.0℃;Reflux; |
2) In a 500 mL four-necked flask equipped with a thermocouple, a stirrer, a water separator, and a reflux condenser,Add an appropriate amount of tetradecanol, toluene (solvent), hydroquinone (polymerization inhibitor), and p-toluenesulfonic acid (catalyst), and heat them to 60C to completely dissolve them.Then add a methacrylic acid so that the molar ratio of methacrylic acid and tetradecanol is 1:1, the amount of toluene is 75% of the total mass of methacrylic acid and tetradecanol, and the amount of hydroquinone is methacrylic acid and The total mass of tetradecanol is 0.5%, and the amount of p-toluenesulfonic acid is 1.0% of the total mass of methacrylic acid and tetradecanol; 3) continue to heat up to the reflux temperature, the water generated by the reaction carried by the water-bearing agent toluene, in the water separator layer;4) When the reaction reaches the theoretical amount of water, the reaction is completed, the reaction is stopped, excess methacrylic acid and toluene are distilled off under reduced pressure, washed with a mass fraction of 5% alkalinity until the lower aqueous layer is colorless, and then saturated NaCl is used. The solution was washed to neutrality and the pH was 7;5) Take an appropriate amount of anhydrous calcium chloride to dry the product, suction filtration, and vacuum drying in a vacuum oven for more than 48 hours to obtain pure tetradecyl methacrylate. |