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CAS No. : | 255727-66-3 | MDL No. : | MFCD16621496 |
Formula : | C15H27BrO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | RHLOSBPISIVGMQ-UHFFFAOYSA-N |
M.W : | 319.28 | Pubchem ID : | 23113089 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
91% | With pyridine In tetrahydrofuran at 0 - 20℃; | |
82.5% | Stage #1: 2-bromoisobutyric acid bromide; 10-Undecen-1-ol With pyridine In tetrahydrofuran for 0.166667h; Stage #2: In tetrahydrofuran at 20℃; Inert atmosphere; | |
75% | With triethylamine In dichloromethane at 0 - 20℃; for 26h; Schlenk technique; Inert atmosphere; |
64% | With pyridine In tetrahydrofuran at 20℃; Schlenk technique; Inert atmosphere; Cooling with ice; | |
With pyridine In tetrahydrofuran | ||
With pyridine In tetrahydrofuran at 20℃; Inert atmosphere; Schlenk technique; | ||
With pyridine In tetrahydrofuran at 20℃; Inert atmosphere; Schlenk technique; |