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[ CAS No. 25812-80-0 ]

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Chemical Structure| 25812-80-0
Chemical Structure| 25812-80-0
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CAS No. :25812-80-0 MDL No. :MFCD00463506
Formula : C8H6Br2O2 Boiling Point : 314.3°C at 760 mmHg
Linear Structure Formula :- InChI Key :N/A
M.W :293.94 g/mol Pubchem ID :2754502
Synonyms :

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Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 25812-80-0 ]

  • Upstream synthesis route of [ 25812-80-0 ]
  • Downstream synthetic route of [ 25812-80-0 ]

[ 25812-80-0 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 493-09-4 ]
  • [ 25812-80-0 ]
YieldReaction ConditionsOperation in experiment
78% With iodine pentoxide; potassium bromide In water at 20℃; for 23 h; General procedure: A mixture of arene (0.5 mmol), I2O5 (334 mg, 1.0 mmol), and KBr (148 mg, 1.25 mmol) was dissolved in 2mL of H2O. The reaction was complete after stirring for the indicated time at room temperature. The mixture was extracted by ethyl acetate and concentrated under reduced pressure, and the mixture was purified by flash column chromatography (silica gel) to afford the desired product.
Reference: [1] Tetrahedron, 2004, vol. 60, # 40, p. 8899 - 8912
[2] European Journal of Organic Chemistry, 2012, # 33, p. 6586 - 6593
[3] Synthetic Communications, 2014, vol. 44, # 2, p. 181 - 187
[4] Tetrahedron, 2007, vol. 63, # 51, p. 12621 - 12628
[5] Journal of the Chemical Society, 1915, vol. 107, p. 1595
[6] Organic Process Research and Development, 2001, vol. 5, # 2, p. 116 - 121
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