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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 26389-68-4 Chemical Structure| 26389-68-4

Structure of 26389-68-4

Chemical Structure| 26389-68-4

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Product Details of [ 26389-68-4 ]

CAS No. :26389-68-4
Formula : C8H15N
M.W : 125.21
SMILES Code : C1(CNCC2CC2)CC1
MDL No. :MFCD12138694

Safety of [ 26389-68-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H226-H335-H314
Precautionary Statements:P210-P240-P241-P242-P243-P260-P264-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P370+P378-P403+P233-P403+P235-P405-P501
Class:3(8)
UN#:2733
Packing Group:

Application In Synthesis of [ 26389-68-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 26389-68-4 ]

[ 26389-68-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 26389-68-4 ]
  • [ 161957-56-8 ]
  • 3-bromo-N,N-bis-(cyclopropylmethyl)-2-fluoro-benzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; for 3h; 8a) 3-Bromo-N,N-bis-cyclopropylmethyl-2-fluoro-benzamide A solution of 3-bromo-2-fluoro-benzoic acid (0.500 g, 2.28 mmol), HATU (0.868 g, 2.28 mmol), N,N-bis-cyclopropylmethylamine (0.329 g, 2.63 mmol) and DIPEA (0.590 g, 4.57 mmol) in DCM (15 ml_) was stirred for 3 h. The mixture was washed with aqueous NaHC03 and dried by passage through a phase separation cartridge. Concentration to dryness gave the crude product (0.904g, quantative), used without further purification. LC-MS m/z 326 (M + H) +, 1 .46 (ret. time), basic method.
 

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