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CAS No. : | 265328-14-1 | MDL No. : | MFCD00662808 |
Formula : | C8H9ClN2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 200.62 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
84% | With sodium hydroxide In tetrahydrofuran |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
14% | With trichlorophosphate at 115℃; for 1h; | |
With trichlorophosphate |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 84 percent / aq. NaOH / tetrahydrofuran 2: (COCl)2 / CH2Cl2 / 0.5 h / 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: 84 percent / aq. NaOH / tetrahydrofuran 2: (COCl)2 / CH2Cl2 / 0.5 h / 20 °C 3: Amberlyst A-21 / ethyl acetate / 1 h / 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / water; ethanol / 16 h / 90 °C 2: trichlorophosphate / 1 h / 115 °C |