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[ CAS No. 26819-10-3 ]

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Chemical Structure| 26819-10-3
Chemical Structure| 26819-10-3
Structure of 26819-10-3 * Storage: {[proInfo.prStorage]}

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Product Details of [ 26819-10-3 ]

CAS No. :26819-10-3 MDL No. :MFCD01215180
Formula : C9H10BrNO Boiling Point : 329.9°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :228.09 g/mol Pubchem ID :-
Synonyms :

Safety of [ 26819-10-3 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:
Hazard Statements:H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 26819-10-3 ]

  • Downstream synthetic route of [ 26819-10-3 ]

[ 26819-10-3 ] Synthesis Path-Downstream   1~14

  • 1
  • [ 88-04-0 ]
  • [ 26819-10-3 ]
  • [ 65262-67-1 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; copper(l) chloride In N,N-dimethyl-formamide Heating;
  • 2
  • [ 95-57-8 ]
  • [ 26819-10-3 ]
  • [ 65262-23-9 ]
YieldReaction ConditionsOperation in experiment
In N,N-dimethyl-formamide Heating;
  • 3
  • [ 1570-64-5 ]
  • [ 26819-10-3 ]
  • [ 65262-58-0 ]
YieldReaction ConditionsOperation in experiment
With copper(l) chloride In N,N-dimethyl-formamide Heating;
  • 4
  • [ 65262-96-6 ]
  • [ 26819-10-3 ]
  • [ 65262-76-2 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate In N,N-dimethyl-formamide Heating;
  • 5
  • [ 26819-10-3 ]
  • [ 113948-01-9 ]
YieldReaction ConditionsOperation in experiment
99% With water-d2 In pyridine; dichloromethane for 24h;
  • 6
  • [ 1711-09-7 ]
  • [ 75-04-7 ]
  • [ 26819-10-3 ]
YieldReaction ConditionsOperation in experiment
41% With sodium hydroxide In dichloromethane; water at 0℃; for 0.5h;
  • 7
  • [ 113948-01-9 ]
  • [ 26819-10-3 ]
  • [ 113948-08-6 ]
YieldReaction ConditionsOperation in experiment
With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
  • 8
  • [ 153409-85-9 ]
  • [ 26819-10-3 ]
  • [ 80031-02-3 ]
YieldReaction ConditionsOperation in experiment
1: 5% 2: 40% With n-butyllithium
YieldReaction ConditionsOperation in experiment
m-Brombenzoylchlorid, Ethylamin;
Entspr. Saeurechlorid, geeignetes Amin, sd. wfr. Bzl.;
  • 10
  • [ 610-71-9 ]
  • [ 26819-10-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: SOCl2 / 4 h / Heating 2: aq. NaOH / CH2Cl2 / 0.5 h 3: 40 percent / n-BuLi
  • 11
  • [ 59615-13-3 ]
  • [ 26819-10-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: aq. NaOH / CH2Cl2 / 0.5 h 2: 40 percent / n-BuLi
  • 12
  • [ 585-76-2 ]
  • [ 26819-10-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: thionyl chloride / 2 h / Heating 2: 41 percent / 10percent NaOH / CH2Cl2; H2O / 0.5 h / 0 °C
  • 13
  • [ 26819-10-3 ]
  • [ 113948-08-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 99 percent / D2O / CH2Cl2; pyridine / 24 h 2: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C
  • 14
  • [ 1711-09-7 ]
  • [ 557-66-4 ]
  • [ 26819-10-3 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide In methanol (50 ml)-water; ethyl acetate 47.i (i) (i) Production of 3-bromo-N-ethylbenzamide To a solution of sodium hydroxide (3.80 g) in methanol (50 ml)-water (15 ml) was added by portions ethylamine hydrochloride (7.80 g) at 0° C. and the mixture was stirred for 5 min. 3-Bromobenzoyl chloride (5.53 g) was added dropwise and the mixture was stirrd at room temperature for 1 h. Methanol was evaporated under reduced pressure, and ethyl acetate was added to the residue for partitioning. The organic layer was washed with water and brine, dried (magnesium sulfate) and concentrated under reduced pressure. The residue was recrystallized from hexane-ethyl acetate to give the title compound (5.47 g) as colorless powder crystals. 1H-NMR (CDCl3) δ: 1.26 (3H, t, J=7.1 Hz), 3.40-3.59 (2H, m), 6.11 (1H, brs), 7.30 (1H, t, J=8.2 Hz), 7.57-7.72 (2H, m), 7.90 (1H, t, J=1.4 Hz). IR (KBr): 3308, 1638, 1541 cm-1.
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