Home Cart Sign in  
Chemical Structure| 273401-26-6 Chemical Structure| 273401-26-6

Structure of 273401-26-6

Chemical Structure| 273401-26-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 273401-26-6 ]

CAS No. :273401-26-6
Formula : C9H9FN2O3
M.W : 212.18
SMILES Code : CC(NC1=CC([N+]([O-])=O)=C(F)C=C1C)=O
MDL No. :MFCD24038777

Safety of [ 273401-26-6 ]

Application In Synthesis of [ 273401-26-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 273401-26-6 ]

[ 273401-26-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 326-65-8 ]
  • [ 273401-26-6 ]
YieldReaction ConditionsOperation in experiment
75% With potassium nitrate; In sulfuric acid; Referential Example 1 4-Fluoro-2-methyl-5-nitroacetanilide To a solution of 4-fluoro-2-methylacetanilide (46.5 g, 278 mmol) in concentrated sulfuric acid (500 ml) was added dropwise a solution of potassium nitrate (141 g, 1.39 mol) in concentrated sulfuric acid (500 ml) over 2 hours at room temperature. After completion of dropwise addition, the reaction mixture was poured into ice water and the precipitated crystals were collected by filtration. These were washed with water and then air-dried, thereby obtaining 44.5 g of title compound as colorless powder. Yield 75%. 1H-NMR(DMSO-d6, δ): 2.11(3H,s), 2.32(3H,s), 7.50(1H,d,J=12.7 Hz), 8.34(1H,d,J=7.3 Hz), 9.56(1H,brs).
 

Historical Records

Technical Information

Categories