Alternatived Products of [ 2760-35-2 ]
Product Details of [ 2760-35-2 ]
CAS No. : | 2760-35-2 |
MDL No. : | |
Formula : |
C9H10BrNO
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
228.09
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 2760-35-2 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 2760-35-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 2760-35-2 ]
- 1
-
[ 2760-35-2 ]
-
[ 96433-09-9 ]
-
[ 1265678-96-3 ]
- 2
-
[ 2760-35-2 ]
-
[ 33513-42-7 ]
-
[ 113092-96-9 ]
Yield | Reaction Conditions | Operation in experiment |
61% |
With trichlorophosphate at 20 - 85℃; for 4h; |
178
Phosphorous oxychloride (3 mE, excess) was treated with DMF (650 uE, 8.7 mmol, 1.5 eq.) and the solution allowed to return to ambient temperature. N-propionyl208 4-bromoaniline (1.32 g, 5.8 mmol, 1 eq.) was added and themixture heated at 85° C. for 4 h. The hot mixture was pouredonto ice (100 g), stirred until melted, and the solids werecollected by filtration. Washing with water and drying invacuo gave clean 6-bromo-2-chioro-3-methylquinoline (914mg, 6 1%). This intermediate (250 mg, 1.0 mmol) and phenol(3 mmol, 3. eq.) were converted, via Methods 11,3, and 5, tocompound 210(118mg, 42%). [M-H]=278. 1 mlz. Activity: |