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Chemical Structure| 28361-38-8 Chemical Structure| 28361-38-8

Structure of 28361-38-8

Chemical Structure| 28361-38-8

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Product Details of [ 28361-38-8 ]

CAS No. :28361-38-8
Formula : C10H11ClO4S
M.W : 262.71
SMILES Code : CC(C)(S(=O)(C1=CC=C(Cl)C=C1)=O)C(O)=O
MDL No. :MFCD12816687

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Application In Synthesis of [ 28361-38-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 28361-38-8 ]

[ 28361-38-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 28361-38-8 ]
  • [ 62058-03-1 ]
  • C20H26ClNO4S [ No CAS ]
YieldReaction ConditionsOperation in experiment
Example B .3 Preparation of compound 3; A mixture of 2-[(p-chlorophenyl)sulfonyl]-2-methylpropionic acid [28361-38-8] (0.00028 mol) in dichloromethane (5 ml) and DMF (5 ml) was stirred and 1-hydroxy- lH-benzotriazole (O.OOO33 mol) was added. Then the mixture was stirred for 10 minutes and iV-(ethylcarbonimidoyl)-iV,iV-dimethyl-l,3-propanediamine, monohydrochloride [25952-53-8] (O.OOO33 mol) was added. The resulting mixture was stirred for 10 minutes and (lalpha,3alpha,4alpha,5beta,7alpha) -4-aminotricyclo[3.3.1.13'7]decan-l-ol [62058-03-1] (O.OOO33 mol) was added. The reaction mixture was stirred overnight at room temperature and then the solvent was evaporated. The residue was purified by column chromatography over silica gel (eluent: CH2CyCH3OH 98/2). The product fractions were collected and the solvent was evaporated, yielding 0.094 g of compound 3.
 

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