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Chemical Structure| 29043-89-8 Chemical Structure| 29043-89-8

Structure of 29043-89-8

Chemical Structure| 29043-89-8

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Product Details of [ 29043-89-8 ]

CAS No. :29043-89-8
Formula : C6H12O2
M.W : 116.16
SMILES Code : O=CCOCCCC

Safety of [ 29043-89-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H226-H302-H315-H318-H335
Precautionary Statements:P210-P233-P240-P241-P242-P243-P261-P264-P270-P271-P280-P301+P312+P330-P303+P361+P353-P304+P340+P312-P305+P351+P338+P310-P332+P313-P370+P378-P403+P233-P403+P235-P405-P501
Class:3
UN#:1993
Packing Group:

Application In Synthesis of [ 29043-89-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29043-89-8 ]

[ 29043-89-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 29043-89-8 ]
  • [ 3684-12-6 ]
  • [ 120329-58-0 ]
  • C79H23NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
44.1% In chlorobenzene; for 48h;Reflux; A chlorobenzene solution (150 mL) of N-phenyl-2-phenylglycine (112 mg, 0.5 mmol), 3-oxaheptanal (116mg, 1 mmol), and a fullerene (360 mg, 0.5 mmol) washeated under reflux for 48 hours. The reaction product solution was concentratedunder reduced pressure, and the reaction product was purifiedby colunm chromatography (Si02 , hexane:toluene=3:1), thereby obtaining 220.9 mg (44.1 %) of the target product(purity: 99% or more). 1H-NMR (CDC13)o: 0.92 (3H, t, 1=7.2 Hz), 1.38-1.52 (2H, m), 1.52-1.70 (2H, m), 3.30-3.42 (lH, m), 3.42-3.52 (lH, m), 4.20 (lH, d-d, 1=10.0, 1.6 Hz), 4.39 (lH, d-d,1=10.0, 4.4 Hz), 5.85 (lH, d-d, 1=4.4, 1.6 Hz), 6.80 (lH, s),6.96-7.05 (lH, m), 7.10-7.37 (7H, m), 7.70 (2H, d, 1=7.6Hz). MS (FAB) m/z 1002(M+). HRMS calcd forC79H23NO 1001.17796; found 1001.1790.
 

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