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Chemical Structure| 2917-02-4 Chemical Structure| 2917-02-4

Structure of 2917-02-4

Chemical Structure| 2917-02-4

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Product Details of [ 2917-02-4 ]

CAS No. :2917-02-4
Formula : C7H11N3OS
M.W : 185.25
SMILES Code : OC1=NC(SCCC)=NC(N)=C1

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Application In Synthesis of [ 2917-02-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2917-02-4 ]

[ 2917-02-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2033-24-1 ]
  • [ 31680-08-7 ]
  • [ 2917-02-4 ]
  • 2-propylmercapto-5-(4-methoxy-3-nitrophenyl)-5,8-dihydropyridino[2,3-d]pyrimidine-4,7(3H,6H)-dione [ No CAS ]
YieldReaction ConditionsOperation in experiment
17.9% In ethylene glycol; at 200℃; for 5h; The 2-propanemercapto-6-aminopyrimidine-4(3H)-one (185mg, 1.0mmol), 2,2-dimethyl-1,3-dioxane-4,6-dione (173mg, 1.2mmol) and 4-Methoxy-3-nitrobenzaldehyde (181mg, 1.0mmol) was dissolved in about 5mL of ethylene glycol, and the reaction was heated at 200C in an oil bath for about 5 hours, TLC (petroleum ether/ethyl acetate = 1/ 2) The point of detecting raw material disappears. Pour the reaction liquid into an appropriate amount of ice water, flocculent precipitation is formed, filtered to obtain a crude product. After separation and purification by a flash column (dichloromethane/methanol: 1.5%), 70 mg of pure product was obtained, and the yield was 17.9%.
 

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