There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 295328-85-7 | MDL No. : | MFCD07772442 |
Formula : | C16H17N | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | NAOGHMNKMJMMNQ-HOTGVXAUSA-N |
M.W : | 223.31 | Pubchem ID : | 11117676 |
Synonyms : |
|
Signal Word: | Danger | Class: | 9 |
Precautionary Statements: | P264-P270-P273-P280-P301+P312+P330-P302+P352+P312-P305+P351+P338+P310-P332+P313-P391-P501 | UN#: | 3077 |
Hazard Statements: | H302+H312-H315-H318-H411 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
81% | With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20℃; for 12h;Inert atmosphere; | General procedure: To a stirred solution of acid 12 (1.0 eq., 0.24 mmol, 50 mg) in dichloromethane(1 mL) at room temperature was added sequentially EDCI (1.4 eq., 0.34 mmol, 65mg), HOAt (1.4 eq., 0.34 mmol, 46 mg), R1R2NH (2.0 eq.,0.48 mmol) and Et3N (3.0 eq., 0.72 mmol, 0.1 mL) and stirred at thesame temperature. After 12 hours, the reaction mixture was extracted with etherand washed with water, brine, dried over Na2SO4 andconcentrated under reduce pressure followed by flash chromatography (SiO2, cyclohexaneto cyclohexane/EtOAc 2/1) to afford amides 21a-f. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
100% | In 2,2,2-trifluoroethanol at 0℃; for 48h; Inert atmosphere; |
A913076[ 155155-73-0 ]
(2R,5R)-2,5-Diphenylpyrrolidine
Reason: Optical isomers
[ 155155-73-0 ]
(2R,5R)-2,5-Diphenylpyrrolidine
Similarity: 1.00
[ 155155-73-0 ]
(2R,5R)-2,5-Diphenylpyrrolidine
Similarity: 1.00