Select Region or Location
Americas
  • Argentina
  • Brazil
  • Canada
  • Mexico
  • United States
  • Other Americas
Europe
  • Austria
  • Belgium
  • Bulgaria
  • Croatia/Hrvatska
  • Cyprus
  • Czech Republic
  • Denmark
  • Estonia
  • Finland
  • France
  • Germany
  • Greece
  • Hungary
  • Ireland
  • Italy
  • Latvia
  • Liechtenstein
  • Lithuania
  • Luxembourg
  • Malta
  • Netherlands
  • Norway
  • Poland
  • Portugal
  • Romania
  • Slovak Republic
  • Slovenia
  • Spain
  • Sweden
  • Switzerland
  • Turkey
  • United Kingdom
  • Other Europe
Asia Pacific
  • Australia
  • China
  • India
  • Indonesia
  • Japan
  • Korea, Republic of
  • Malaysia
  • New Zealand
  • Philippines
  • Singapore
  • Thailand
  • Vietnam
  • Other Asia Pacific
Africa And Middle East
  • Egypt
  • Israel
  • Other Africa And Middle East
USD
Home Cart Sign in  
Chemical Structure| 29911-28-2 Chemical Structure| 29911-28-2

Structure of 29911-28-2

Chemical Structure| 29911-28-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only! Not for Human Use. We Do Not Sell to Patients.

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

DE Stock

US Stock

Asia Stock

Global Stock

In Stock
{[ item.pr_size ]}{[ size_append_text(item.pr_size, proInfo.prAm, 'list') ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

  • {[ item.pr_size ]}
    {[ size_append_text(item.pr_size, proInfo.prAm, 'list') ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 29911-28-2 ]

CAS No. :29911-28-2
Formula : C10H22O3
M.W : 190.28
SMILES Code : CC(OCC(O)C)COCCCC
English Name :1-((1-Butoxypropan-2-yl)oxy)propan-2-ol
MDL No. :MFCD00192112
InChI Key :CUVLMZNMSPJDON-UHFFFAOYSA-N
Pubchem ID :24752

Safety of [ 29911-28-2 ]

Application In Synthesis of [ 29911-28-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29911-28-2 ]

[ 29911-28-2 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 29911-28-2 ]
  • [ 75-36-5 ]
  • [ 2266578-04-3 ]
  • 2
  • [ 75-56-9 ]
  • [ CAS Unavailable ]
  • [ 29911-28-2 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide at 190℃;
  • 3
  • [ CAS Unavailable ]
  • [ 75-56-9 ]
  • [ 29911-28-2 ]
YieldReaction ConditionsOperation in experiment
In butan-1-ol
YieldReaction ConditionsOperation in experiment
Entspr. Propylenoxid, n-Butanol;
  • 5
  • [ 29911-28-2 ]
  • [ 45096-22-8 ]
  • [ CAS Unavailable ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
With phosphorous (V) sulfide In n-heptane at 95 - 118℃; for 8.5h; 12 Example 12 Dithiophosphoric Acid Mixture, Lot RJT-569-56; A three neck round bottom flask was charged with 121.5 grams of phosphorous pentasulfide and 135.4 grams of heptane. This was attached to a scrubber to remove hydrogen sulfide gas. The flask was then flushed with nitrogen gas. To a second round bottom flask was added 226.5 grams of dipropylene glycol monobutyl ether and 95.3 grams of tripropylene glycol. The alcohol mixture was then added to the phosphorous pentasulfide over a period of two hours. The reaction mixture was then heated to 95° C. over a period of three and one half hours. The reaction was heated further, and heptane was removed by distillation. After the temperature reached 118° C., the reaction was heated for an additional three hours. An aspirator was attached to remove any remaining heptane. The final product was then filtered with diatomaceous earth.
  • 6
  • [ 540-54-5 ]
  • [ 29911-28-2 ]
  • [ 41890-72-6 ]
YieldReaction ConditionsOperation in experiment
70% With tetrabutylammomium bromide; potassium hydroxide; sodium hydroxide at 120 - 160℃; for 10h; 6 Example 6: Dipropylene glycol dibutyl ether(DPGDBE)Synthesis of 1 General procedure: In a four-necked flask(1) dipropylene glycol monobutyl ether,(2) n-Butyl chloride,(3) a mixture of sodium hydroxide and potassium hydroxide,(4) tetrabutylammonium bromide in a molar ratio of 1.0: 3.0: 5.0: 0.06, and the mixture was heated and stirred at 120 ° C. to 160 ° C. for 10 hours. Thereafter, it was washed with water and hydrochloric acid to obtain crude DPGDBE.This was purified by distillation to obtain the objective DPGDBE in a purity of 99.0 mass%. The reaction yield was 70%.
  • 7
  • [ 29911-28-2 ]
  • [ 2379894-58-1 ]
YieldReaction ConditionsOperation in experiment
84 g With 2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid In dichloromethane at 0 - 20℃; for 4h; Preparation of l-((l-(Butoxy)-2-propanyl)oxy)-2-propanone (DPnB Ketone): In a fume hood, a 2L Erlenmeyer flask is charged with l-((l-(Butoxy)-2- propanyl)oxy)-2-propanol (225 mL, 1.05 mol), dichloromethane 525 mL), TEMPO (1.64 g, 10.51 mmol) and cooled to 5 °C (temperature was monitored with a thermometer) using an ice bath. Trichloroisocyanuric acid (269.3 g, 1.10 mol) is added in small portions using a spatula over an hour. The mixture is stirred for an additional hour at 0 °C and then warmed to room temperature and stirred for 1 more hour. The mixture is filtered and cooled to 5 °C. 200 mL of saturated aqueous sodium carbonate is added and the organic layer separated. Another 200 mL of saturated aqueous sodium carbonate is added along with 20 mL saturated aqueous sodium sulfite. The organic layer is separated and washed with brine (2 x 600 mL) and dried over magnesium sulfate. After filtering, the mixture is concentrated to a yellowish oil (160 g). The oil is fractionally distilled under vacuum (-1x10-2 torr) to afford a colorless middle fraction (84.0 g, >98% purity as determined by GC analysis).
  • 8
  • [ 29911-28-2 ]
  • [ 3114703-15-7 ]
  • [ 3118108-36-1 ]
YieldReaction ConditionsOperation in experiment
Stage #1: dipropylene glycol monobutyl ether; C25H40N5O8P With 1H-tetrazole In acetonitrile at 30℃; for 2h; Inert atmosphere; Stage #2: With tert.-butylhydroperoxide In decane; acetonitrile at 30℃; for 2h; Inert atmosphere; General procedure: The crude compound 8a-1 (1.0 g, 4 mmol) was added to anhydrous acetonitrile (50mL), and2-hydroxyethyl octanoate (752mg, 4 mmol) was added. The mixture was stirred and dissolved,and a solution of 1H-tetrazolium in acetonitrile (0.45 M, 13.3mL, 6 mmol) was added dropwiseunder an ice bath. The reaction was carried out at 30 ° C for 2 hours under a nitrogen atmosphere.TLC showed that the reaction was complete, and (5.0-6.0M in Decane) tert-butyl hydroperoxidesolution (1.45mL, 8mmol) was added. The reaction was carried out at 30 ° C for 2 hours under anitrogen atmosphere. TLC showed that the reaction was complete, and 30mL of ethyl acetate wasadded to dilute the reaction solution. A saturated aqueous solution of sodium thiosulfate (100mL)was added to quench the mixture, and the mixture was separated. The organic phase was driedover anhydrous sodium sulfate, filtered, and the solvent was removed.
 

Historical Records

Technical Information

Categories