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Chemical Structure| 299441-95-5 Chemical Structure| 299441-95-5

Structure of 299441-95-5

Chemical Structure| 299441-95-5

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Product Details of [ 299441-95-5 ]

CAS No. :299441-95-5
Formula : C9H8BrN3OS
M.W : 286.15
SMILES Code : NC1=NN=C(COC2=CC=C(Br)C=C2)S1
MDL No. :MFCD01043765

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Application In Synthesis of [ 299441-95-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 299441-95-5 ]

[ 299441-95-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1878-91-7 ]
  • [ 79-19-6 ]
  • [ 299441-95-5 ]
YieldReaction ConditionsOperation in experiment
General procedure: A mixture of benzoic acid (50 mmol), N-aminothiourea(50 mmol) and POCl3 (13 mL) was heated at 75 C for 0.5 h. Themixture was cooled to which water (10 mL) was added and thereaction mixture was refluxed for 4 h. The mixture was cooled and pH was adjusted to 8.0 by adding 50% sodium hydroxide solution.The separated solid was filtered and recrystallized from ethanolto give desired compounds.
 

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