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[ CAS No. 30464-83-6 ] {[proInfo.proName]}

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CAS No. :30464-83-6 MDL No. :MFCD12402587
Formula : C10H11NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :PXUQJNBVONMHOX-UHFFFAOYSA-N
M.W : 177.20 Pubchem ID :10821185
Synonyms :

Safety of [ 30464-83-6 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P270-P301+P312-P330-P302+P352-P333+P313-P321-P261-P272-P280-P363-P501 UN#:
Hazard Statements:H302-H317 Packing Group:
GHS Pictogram:

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 30464-83-6 ]

[ 30464-83-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 20538-12-9 ]
  • [ 30464-83-6 ]
YieldReaction ConditionsOperation in experiment
10 g With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 25℃; for 3h; 35A Embodiment 35A
(7-Methoxy-1H-indol-2-yl)methanol
Ethyl-7-methoxy-1H-indole-2-carboxylate (11.00 g, 50.17 mmol) was dissolved in THF (100 mL) at 0 °C and lithium aluminum hydride (2.86 g, 75.26 mmol) was added to the mixture and the reaction mixture was warmed to 25 °C and stirred for 3 hours. LCMS showed the reaction was complete, H2O (1 mL) and NaOH (1 mL) were added to the reaction mixture, then H2O (3 mL) was added, filtered and the filtrate was concentrated to deliver the title compound (brown oil, 10.00 g). 1H NMR (400MHz, CDCl3): δ 8.57 (br. s., 1 H), 7.20 (d, J=8.0 Hz, 1 H), 7.03 (t, J=8.0 Hz, 1 H), 6.65 (d, J=8.0 Hz, 1 H), 6.40 (d, J=4.0 Hz, 1 H), 4.84 (d, J=4.0 Hz, 2 H), 3.97 (s, 3 H). LCMS (ESI) (5-95AB): m/z: 178.1 [M+1].
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