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Chemical Structure| 3096-69-3 Chemical Structure| 3096-69-3

Structure of 3096-69-3

Chemical Structure| 3096-69-3

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Product Details of [ 3096-69-3 ]

CAS No. :3096-69-3
Formula : C8H11NO
M.W : 137.18
SMILES Code : OC1=CC=C(N)C(C)=C1C
MDL No. :MFCD00070554
InChI Key :UBKPLLYABUUFCE-UHFFFAOYSA-N
Pubchem ID :76542

Safety of [ 3096-69-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P280-P305+P351+P338-P310

Application In Synthesis of [ 3096-69-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3096-69-3 ]

[ 3096-69-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 19499-93-5 ]
  • [ 3096-69-3 ]
YieldReaction ConditionsOperation in experiment
97% With hydrogen;palladium 10% on activated carbon; In ethanol; at 20℃; for 5.0h; Synthesis 137; 4-Amino-2,3-dimethylphenol; A mixture of <strong>[19499-93-5]2,3-dimethyl-4-nitrophenol</strong> (2 g, 1.2 mmol) and Pd(C) (10percent) (1.83 g) in EtOH (80 ml_) was stirred at room temperature under H2 atmosphere for 5 hours. The crude mixture was then filtered using celite and washed with DCM. After evaporating the solvent, the title compound (1.60 g, 97percent) was obtained as a brown powder. 1H-NMR (delta, ppm, DMSO-d6): 1.94 (s, 3H, HMe), 2.01 (s, 3H, HMe), 4.06 (s, 2H, NH2), 6.32 (d, 1H, Harom 6, JB-5=8.1 Hz), 6.40 (d, 1H, Harom 5, J6-5=8.1Hz), 6.61 (s, 1H, Harom 2), 8.10 (broad s, 1H, OH).
 

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