Home Cart Sign in  
Chemical Structure| 311-28-4 Chemical Structure| 311-28-4
Chemical Structure| 311-28-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

Synonyms: Tetra-n-butylammonium iodide; TBAI

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of Tetrabutylammonium iodide

CAS No. :311-28-4
Formula : C16H36IN
M.W : 369.37
SMILES Code : [I-].CCCC[N+](CCCC)(CCCC)CCCC
Synonyms :
Tetra-n-butylammonium iodide; TBAI
MDL No. :MFCD00011636
InChI Key :DPKBAXPHAYBPRL-UHFFFAOYSA-M
Pubchem ID :67553

Safety of Tetrabutylammonium iodide

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Tetrabutylammonium iodide

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 311-28-4 ]

[ 311-28-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 311-28-4 ]
  • [ 110-17-8 ]
  • [ 2915-53-9 ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; In chloroform; 1-bromo-hexane; water; Petroleum ether; (ii) Preparation of Hexyl/Octyl Maleate/Fumarate Monooctyl maleic/fumaric acid (88 g, 0.39 mole) was dissolved in chloroform (200 ml) and was stirred in a 1 L Erlenmeyer (Quick Fit) flask, fitted with condenser, with a solution of potassium hydroxide (21 g, 0.38 mole) and tetrabutyl ammonium iodide (15 g, 0.04 mole) in 200 mls of water. To the stirred mixture was added hexyl bromide 64 g, 0.39 mole) and the two phase mixture was stirred rapidly under reflux for 5 hours. The chloroform layer was separated off, washed with sodium carbonate solution, then with water, and then dried over sodium sulphate. After filtering and evaporating the resulting oil was treated with 30/40 petroleum ether which precipitated the catalyst which could be reused. Filtration/evaporation yielded the crude product as an oil (77 g). Distillation in vacuo removed 13.1 g hexyl bromide. The yield of undistilled material was 59.3 g (62percent based on hexyl bromide).
 

Historical Records

Categories