There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 31645-35-9 | MDL No. : | MFCD00673247 |
Formula : | C19H16O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | MJYSISMEPNOHEG-UHFFFAOYSA-N |
M.W : | 276.33 | Pubchem ID : | 3618754 |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P280-P305+P351+P338-P310 | UN#: | 1759 |
Hazard Statements: | H318 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
98% | With triethylamine In dichloromethane at 0 - 20℃; | |
90% | With triethylamine at 20℃; | 2.3. Synthesis of Fluorophore-ContainingMethacrylate Monomers (AntMA: 1 andPyMA: 2) 9-Anthracenemethanol (4.5 g; 0.022 mol) was addedto a solution of triethylamine (9.0 mL; 0.065 mol) in250 mL of anhydrous MC. Methacryloyl chloride (6.3 mL;0.065 mol) was added dropwise under stirring at 0 C.The reaction was then conducted at room temperatureovernight, after which the reaction medium was filtered.The solvent was evaporated, and the solid residue waspurified by recrystallization in 95% ethanol at 40 C(yield = 90%). 1H NMR (CDCl3, ppm: 7.45-8.50(m, 9H, aromatic H), 6.20 (s, 2H, CH2O), 6.05 (s, 1H,CH2= C), 5.56 (s, 1H, CH2= C), 1.97 (s, 3H, CH3 . |
80% | With dmap; triethylamine In dichloromethane at 0℃; for 4.5h; Inert atmosphere; |
73% | With pyridine; dmap In chloroform at 0 - 20℃; for 4h; | |
70% | With 4-t-butyl-o-xylene; triethylamine In chloroform at 20℃; Cooling with ice; | |
70% | Stage #1: 9-hydroxymethylanthracene With triethylamine In tetrahydrofuran for 0.5h; Cooling with ice; Stage #2: Methacryloyl chloride In tetrahydrofuran at 0 - 20℃; | |
65% | With triethylamine In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Darkness; | |
42% | With pyridine; triethylamine In tetrahydrofuran at 0 - 20℃; for 1h; | |
In tetrahydrofuran for 0.75h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
9-Chlormethylanthracen, 1.) CH2=C(CH3)-COOH, 80-85grad, 2.) CH3CN, (C2H5)3N; | ||
9-Anthryldiazomethan, Methacrylsaeure; | ||
9-Anthryldiazomethan, Methacrylsaeure, in Petrolether, ZT; |
9-Anthryl-diazomethan, Methacrylsaeure (S.1263); | ||
aus 9-anthryldiazomethane, methacrylsaeure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In toluene at 60℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With dibenzoyl peroxide In toluene at 99.85 - 104.85℃; for 24h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With 2,2'-azobis(isobutyronitrile) In N,N-dimethyl-formamide at 80℃; for 48h; Schlenk technique; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70% | With dmap; dicyclohexyl-carbodiimide In acetonitrile for 24h; Inert atmosphere; |
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