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CAS No. : | 31786-46-6 | MDL No. : | MFCD14697992 |
Formula : | C9H9BrO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | LPZDOTAGNAUWRS-UHFFFAOYSA-N |
M.W : | 245.07 | Pubchem ID : | 13940770 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | With potassium carbonate In N,N-dimethyl-formamide at 20℃; | To a mixture of 2-bromo-6-methoxybenzoic acid (40 g, 0.176 mol) in DMF (300 mL) was added K2CO3 (24.8 g, 0.176 mol) and CH3I (37 g, 0.264 mol). The mixture was stirred at RT overnight. The reaction was quenched with 1M HCl aq and the mixture was extracted with EtOAc (3*300 mL). The organic phase was dried over MgSO4 and concentrated in vacuo to give the title compound (41 g, 99percent). |