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Chemical Structure| 32464-55-4 Chemical Structure| 32464-55-4

Structure of 32464-55-4

Chemical Structure| 32464-55-4

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Product Details of [ 32464-55-4 ]

CAS No. :32464-55-4
Formula : C16H21NO4
M.W : 291.34
SMILES Code : O=C1N(CCCC(OCC)OCC)C(C2=C1C=CC=C2)=O
MDL No. :MFCD09923598
Boiling Point : No data available

Safety of [ 32464-55-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 32464-55-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 32464-55-4 ]

[ 32464-55-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 179543-88-5 ]
  • [ 32464-55-4 ]
  • [ 1432472-67-7 ]
YieldReaction ConditionsOperation in experiment
88% With sulfuric acid; In water; at 95℃; for 2h; [0494] The N-phthaloyl protected 5-methoxy-4-azaindole was prepared by heating the 5- hydrazinyl-2-methoxypyridine hydrochloride (502 mg, 2.86 mmole) and 2-(4,4- diethoxybutyl)isoindoline-l,3-dione (1 g, 3.43 mmole) in 50 mL of 4 % sulfuric acid and 8 mL ethanol at 95 oC for 2 h in a 250 mL round bottom flask. The reaction mixture was cooled to 25 oC and neutralized with 30 % NH40H. The reaction mixture was extracted with EtOAc (1 x 20 mL) and washed with water and brine. The organic layer was dried over Na2S04 and solvent evaporated to obtain 820 mg of product as pale brown solid. Yield: 88 %.
 

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