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Chemical Structure| 326024-05-9 Chemical Structure| 326024-05-9

Structure of 326024-05-9

Chemical Structure| 326024-05-9

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Product Details of [ 326024-05-9 ]

CAS No. :326024-05-9
Formula : C11H13NO5S
M.W : 271.29
SMILES Code : O=C(O)C1=CC(S(=O)(N2CCCC2)=O)=CC=C1O
MDL No. :MFCD02700702

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 326024-05-9 ]

[ 326024-05-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 123-75-1 ]
  • [ 17243-13-9 ]
  • [ 326024-05-9 ]
YieldReaction ConditionsOperation in experiment
EXAMPLE 63 2-Ethoxy-5-(pyrrolidine-1-sulfonyl)benzoic acid ethyl ester A solution of <strong>[17243-13-9]5-chlorosulfonyl-2-hydroxybenzoic acid</strong> (0.52 g, 2.0 mmol, Matrix Scientific) in tetrahydrofuran (10 mL) was treated with pyrrolidine (1.5 g, 21 mmol) and refluxed for 2 h. This was cooled and poured into dilute aqueous hydrochloric acid and extracted into dichloromethane (2*50 mL). The combined extracts were washed with brine, dried over magnesium sulfate, filtered, and concentrated to give a solid. This was triturated with ether to give 2-hydroxy-5-(pyrrolidine-1-sulfonyl)benzoic acid as a solid. _
 

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