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[ CAS No. 32938-44-6 ]

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2D
Chemical Structure| 32938-44-6
Chemical Structure| 32938-44-6
Structure of 32938-44-6 *Storage: {[proInfo.prStorage]}

Quality Control of [ 32938-44-6 ]

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Related Doc. of [ 32938-44-6 ]

SDS

Product Details of [ 32938-44-6 ]

CAS No. :32938-44-6MDL No. :MFCD11617090
Formula :C6H6Br3NBoiling Point :-
Linear Structure Formula :-InChI Key :-
M.W :331.83Pubchem ID :71720973
Synonyms :

Computed Properties of [ 32938-44-6 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 32938-44-6 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 32938-44-6 ]

  • Downstream synthetic route of [ 32938-44-6 ]

[ 32938-44-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 187235-08-1 ]
  • [ 32938-44-6 ]
  • [ 1188334-71-5 ]
  • 2
  • [ 118289-16-0 ]
  • [ 32938-44-6 ]
YieldReaction ConditionsOperation in experiment
79% With dibromo sulfoxide; In dichloromethane; at 0℃; (2-Bromo-4- pyridyl)methanol (2.00 g, 10.6 mmol) was dissolved in dry CH2Cl2 (10 mL) and then SOBr2 (0.90 mL, 11.7 mmol) was added at 00C. The reaction mixture was stirred overnight, then the solvent was evaporated and the residue crystallised from MeOH-Et2O to give the title compound (2.81 g, 79 %) as a white solid. APCI MS m/z 252.2 (M + H). 1H-NMR (400 MHz, (CD3)2SO) delta 8.39 (d, J= 5.0 Hz, IH), 7.74 (d, J= 0.9 Hz, IH), 7.51 (dd, J- 5.0, 1.4 Hz, IH), 4.66 (s, 2H).
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[ 32938-44-6 ]

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