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[ CAS No. 330550-92-0 ] {[proInfo.proName]}

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Chemical Structure| 330550-92-0
Chemical Structure| 330550-92-0
Structure of 330550-92-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 330550-92-0 ]

CAS No. :330550-92-0 MDL No. :MFCD07440225
Formula : C9H11ClN4O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 242.66 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 330550-92-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 330550-92-0 ]

[ 330550-92-0 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 330550-92-0 ]
  • [ 51013-67-3 ]
  • [ 1350545-51-5 ]
YieldReaction ConditionsOperation in experiment
80.6% In butan-1-ol; at 90℃; for 4h; 4-morpholinomethylphenylamine(3.8g) was added to a solution of Compound 2-5(4.8g) in n-butanol(150ml). The mixture was reacted at 90C for 4.0 hours, cooled to room temperature, filtered, washed and dried to obtain a yellow solid(6.3g) in a yield of 80.6%. MS m/z(ESI): 399[M+H]+.
  • 2
  • [ 330550-92-0 ]
  • [ 33311-29-4 ]
  • [ 1350545-52-6 ]
YieldReaction ConditionsOperation in experiment
80.9% In butan-1-ol; at 90℃; for 4h; <strong>[33311-29-4]4-(2-methoxyethoxy)phenylamine</strong>(2.7g) was added to a solution of Compound 2-5(3.7g) in n-butanol(80ml). The mixture was reacted at 90C for 4.0 hours, cooled to room temperature, filtered, washed and dried to obtain a yellow floc-like solid(4.53g) in a yield of 80.9%. MS m/z(ESI): 374[M+H]+; 1H NMR(400 MHz, DMSO-d6): delta10.34(s, 1H), 8.95(s, 1H), 8.50(s, 1H), 7.70(d, J=6.0Hz, 2H), 6.93(d, J=8.8Hz, 2H), 4.43(m, 1H), 4.07(m, 2H), 3.64(m, 2H), 3.30(s, 3H), 2.03(m, 2H), 1.72(m, 2H), 1.61(m, 4H)ppm.
  • 3
  • [ 330550-92-0 ]
  • [ 611225-86-6 ]
  • [ 1350545-53-7 ]
YieldReaction ConditionsOperation in experiment
81.8% In butan-1-ol; at 90℃; for 4h; <strong>[611225-86-6]4-((4-ethylpiperazin-1-yl)methyl)phenylamine</strong>(3.6g) was added to a solution of Compound 2-5(6.0g) in n-butanol(130ml). The mixture was reacted at 90C for 4.0 hours, cooled to room temperature, filtered, washed and dried to obtain a red solid in a yield of 81.8%. MS m/z(ESI): 426[M+H]+.
  • 4
  • [ 330550-92-0 ]
  • [ 70261-82-4 ]
  • [ 1350545-54-8 ]
YieldReaction ConditionsOperation in experiment
85.7% In butan-1-ol; at 90℃; for 4h; <strong>[70261-82-4]4-((4-methylpiperazin-1-yl)methyl)phenylamine</strong>(4.7g) was added to a solution of Compound 2-5(5.28g) in n-butanol(130ml). The mixture was reacted at 90C for 4.0 hours, cooled to room temperature, filtered, washed and dried to obtain a red solid in a yield of 85.7%. MS m/z(ESI): 412[M+H]+.
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