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Chemical Structure| 34108-13-9 Chemical Structure| 34108-13-9

Structure of 34108-13-9

Chemical Structure| 34108-13-9

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Product Details of [ 34108-13-9 ]

CAS No. :34108-13-9
Formula : C17H13NO3
M.W : 279.29
SMILES Code : O=C(OC(C1=CC=C(OC)C=C1)=N/2)C2=C\C3=CC=CC=C3

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Application In Synthesis of [ 34108-13-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34108-13-9 ]

[ 34108-13-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 100-52-7 ]
  • [ 13214-64-7 ]
  • [ 34108-13-9 ]
YieldReaction ConditionsOperation in experiment
86.3% 1.20 g d, 6.89 mmol AcONa was added to a 100 mL two-necked flask,Vacuum, nitrogen protection, then add 20mL of Ac2O,Room temperature stirring for half an hour, then add benzaldehyde 5.74mmol,Heating to 60 , heating reaction 4h; cooling toThe contents of the flask were transferred to a beaker at room temperature, about 120 mL of water was added,Room temperature stirring 3h, precipitation of yellow solid, filter,A small amount of water, dry under the infrared light, the yellow solid product e 1.39g,Yield: 86.3percent.
  • 2
  • [ 100-52-7 ]
  • [ 13214-64-7 ]
  • [ 34108-13-9 ]
 

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