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Chemical Structure| 35424-56-7 Chemical Structure| 35424-56-7

Structure of 35424-56-7

Chemical Structure| 35424-56-7

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Product Details of [ 35424-56-7 ]

CAS No. :35424-56-7
Formula : C7H6ClI
M.W : 252.48
SMILES Code : ICC1=CC=C(Cl)C=C1
MDL No. :MFCD00971975

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Application In Synthesis of [ 35424-56-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 35424-56-7 ]

[ 35424-56-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 108-10-1 ]
  • [ 35424-56-7 ]
  • [ 22916-47-8 ]
  • [ 57265-35-7 ]
YieldReaction ConditionsOperation in experiment
In dichloromethane; di-isopropyl ether; EXAMPLE X 4.2 Parts of 1-[2,4-dichloro-beta-(2,4-dichlorobenzyloxy)-phenethyl]imidazole, 3.7 parts of p-chlorobenzyl iodide and 56 parts of methylene chloride are mixed together and stirred at reflux temperature for 5 hours to obtain a 1-(p-chlorobenzyl)-3-[2,4-dichlorobeta-(2,4-dichlorobenzyloxy)phenethyl imidazolium iodide product which remains in the reaction mixture. The reaction mixture is warmed to evaporate off the solvent and to recover the product as residue. The crude product is purified by washing with 2-propanol and crystallizing from a mixture of 4-methyl-2-pentanone and diisopropyl ether, to yield 1-(p-chlorobenzyl)-3-[2,4-dichloro-beta-(2,4-dichlorobenzyloxy)phenethyl]imidazolium iodide; m.p. 145°- 148° C.
 

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