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[ CAS No. 35681-40-4 ]

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2D
Chemical Structure| 35681-40-4
Chemical Structure| 35681-40-4
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Product Details of [ 35681-40-4 ]

CAS No. :35681-40-4MDL No. :MFCD01067639
Formula : C10H12N2O Boiling Point : -
Linear Structure Formula :-InChI Key :-
M.W :176.22Pubchem ID :-
Synonyms :

Computed Properties of [ 35681-40-4 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

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Application In Synthesis of [ 35681-40-4 ]

  • Downstream synthetic route of [ 35681-40-4 ]

[ 35681-40-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 52099-72-6 ]
  • [ 35681-40-4 ]
YieldReaction ConditionsOperation in experiment
6.97 g (100%) palladium; In methanol; 1-Isopropyl-1,3-dihydro-benzoimidazol-2-one A mixture of 1-isopropenyl-1,3-dihydro-benzoimidazol-2-one (J. Davoll, J. Chem. Soc. 1960, 308) (6.90 g, 39.6 mmol) and 10% palladium on carbon (1.0 g) in MeOH (50 mL) was placed in a Parr shaker under hydrogen (40 psi) for 2 h. The reaction mixture was filtered through celite and evaporated to give 6.97 g (100%) of 1-isopropyl-1,3-dihydro-benzoimidazol-2-one as a white solid. 1H NMR (CDCl3) delta 1.57 (d, J=7.1 Hz, 6H), 4.70-4.81 (m, 1H), 7.02-7.10 (m, 2H), 7.10-7.20 (m, 2H); MS m/e 177 (MH+); Anal. Calcd for C10H12N2O: C, 68.16; H, 6.86; N, 15.90; Found: C, 68.05; H, 6.63; N, 15.77.
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