Alternatived Products of [ 35681-40-4 ]
Alternatived Products of [ 35681-40-4 ]
Product Details of [ 35681-40-4 ]
CAS No. : | 35681-40-4 | MDL No. : | MFCD01067639 |
Formula : |
C10H12N2O
|
Boiling Point : |
- |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 176.22 | Pubchem ID : | - |
Synonyms : |
|
Computed Properties of [ 35681-40-4 ]
TPSA :Topological Polar Surface Area |
- |
H-Bond Acceptor Count : |
- |
XLogP3 : |
- |
H-Bond Donor Count : |
- |
SP3 : |
- |
Rotatable Bond Count : |
- |
Safety of [ 35681-40-4 ]
Signal Word: | | Class: | |
Precautionary Statements: | | UN#: | |
Hazard Statements: | | Packing Group: | |
Application In Synthesis of [ 35681-40-4 ]
- Downstream synthetic route of [ 35681-40-4 ]
- 1
-
[ 52099-72-6 ]

-
[ 35681-40-4 ]
Yield | Reaction Conditions | Operation in experiment |
6.97 g (100%) |
palladium; In methanol; |
1-Isopropyl-1,3-dihydro-benzoimidazol-2-one A mixture of 1-isopropenyl-1,3-dihydro-benzoimidazol-2-one (J. Davoll, J. Chem. Soc. 1960, 308) (6.90 g, 39.6 mmol) and 10% palladium on carbon (1.0 g) in MeOH (50 mL) was placed in a Parr shaker under hydrogen (40 psi) for 2 h. The reaction mixture was filtered through celite and evaporated to give 6.97 g (100%) of 1-isopropyl-1,3-dihydro-benzoimidazol-2-one as a white solid. 1H NMR (CDCl3) delta 1.57 (d, J=7.1 Hz, 6H), 4.70-4.81 (m, 1H), 7.02-7.10 (m, 2H), 7.10-7.20 (m, 2H); MS m/e 177 (MH+); Anal. Calcd for C10H12N2O: C, 68.16; H, 6.86; N, 15.90; Found: C, 68.05; H, 6.63; N, 15.77. |