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[ CAS No. 35754-37-1 ] {[proInfo.proName]}

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Chemical Structure| 35754-37-1
Chemical Structure| 35754-37-1
Structure of 35754-37-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 35754-37-1 ]

CAS No. :35754-37-1 MDL No. :MFCD28786244
Formula : C6H2Cl2FNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 209.99 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 35754-37-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 35754-37-1 ]

[ 35754-37-1 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 35754-37-1 ]
  • [ 2729-36-4 ]
YieldReaction ConditionsOperation in experiment
4 g With iron; ammonium chloride In ethanol; water at 85℃; for 1 h; l,2-dichloro-3-fluoro-5-nitro-benzene (5 g, 23.8 mmol), NH4C1 (14 g, 261.9 mmol) was dissolved in EtOH/H2O(160 mL, 15/1). The solution heated to 85°C followed by addition of Fe in portions. After additon the reaction mixture was heated( 85°C) for lh. The reaction mixture was extracted with EtOAc (10 mL x 3). The combined organic layers were washed with brine (15 mL), dried over Na2S04, and concentrated in vacuum to give crude product. Purification by flash chromatography gave 3,4- dichloro-5-fluoro-aniline (4 g).
Reference: [1] Patent: WO2016/120403, 2016, A1, . Location in patent: Page/Page column 200
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