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Chemical Structure| 358665-70-0 Chemical Structure| 358665-70-0

Structure of 358665-70-0

Chemical Structure| 358665-70-0

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Product Details of [ 358665-70-0 ]

CAS No. :358665-70-0
Formula : C9H12BrNO3S
M.W : 294.17
SMILES Code : O=S(C1=CC=C(OC)C(Br)=C1)(N(C)C)=O
MDL No. :MFCD02135261

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 358665-70-0 ]

[ 358665-70-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 23094-96-4 ]
  • [ 124-40-3 ]
  • [ 358665-70-0 ]
YieldReaction ConditionsOperation in experiment
66% In tetrahydrofuran; for 0.5h;Heating / reflux; Combine <strong>[23094-96-4]3-bromo-4-methoxybenzenesulfonyl chloride</strong> (l. Og, 3.5 mmol) and dimethylamine (8.75 ml of 1M solution in THF, 8.75 mmol) in 25 ml anhydrous THF and heat under reflux in a nitrogen atmosphere for 30 minutes. Concentrate the cooled mixture in vacuo and partition the residue between ethyl acetate and water. Wash the organic layer with 0.1 N HC1 solution, 0.1 N NaOH solution and brine and dry over anhydrous sodium sulfate. Evaporate the solvent and recrystallize the crude solid from ethyl acetate/hexane to yield the title compound (680 mg, 66% yield).
 

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