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CAS No. : | 36394-75-9 | MDL No. : | MFCD00145252 |
Formula : | C5H7ClO3 | Boiling Point : | - |
Linear Structure Formula : | ClCOCH(CH3)OCOCH3 | InChI Key : | ALHZEIINTQJLOT-VKHMYHEASA-N |
M.W : | 150.56 | Pubchem ID : | 11094804 |
Synonyms : |
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Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P261-P264-P270-P272-P280-P301+P312-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P321-P333+P313-P363-P405-P501 | UN#: | 3265 |
Hazard Statements: | H302-H314-H317 | Packing Group: | Ⅱ |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92% | In diethyl ether; at -10 - 20℃; for 3h; | To a stirred suspension of S-<strong>[117324-58-0]methyl 2-amino-5-trifluoromethylbenzoate</strong> (4.2 g, 19.2 mmol) in diethyl ether (300 mL), compound 3(11.56 g, 76.8 mmol) was added dropwise at - 10-0C. The reaction mixture was stirred at room temperature for 3h. After the completion of reaction (monitored by TLC), mixture was washed with hydrochloric acid, water, NaHCO3 solution,and aqueous saturated sodium chloride then dried over Na2SO4. The dried extract was filtered and concentrated under reduced pressure to give S-methyl 2-(2-acetoxypropionyl amino)-5-trifluoromethyl benzoate compound 4 (5.87 g, 92.0%). |