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[ CAS No. 375358-19-3 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 375358-19-3
Chemical Structure| 375358-19-3
Chemical Structure| 375358-19-3
Structure of 375358-19-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 375358-19-3 ]

CAS No. :375358-19-3 MDL No. :MFCD02238180
Formula : C9H6ClNO Boiling Point : -
Linear Structure Formula :- InChI Key :OKRDYODLCPEIMP-UHFFFAOYSA-N
M.W : 179.60 Pubchem ID :135427710
Synonyms :

Safety of [ 375358-19-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 375358-19-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 375358-19-3 ]
  • Downstream synthetic route of [ 375358-19-3 ]

[ 375358-19-3 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 375358-19-3 ]
  • [ 74-88-4 ]
  • [ 49609-15-6 ]
YieldReaction ConditionsOperation in experiment
96% With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 12 h; Intermediate 441 (2.5 g, 13.9 mmol, 1 .0 eq ) was dissolved in DMF (25 mL), 2CO3 (5.76 g, 4 1 .76 mmol, 3 eq ) and CH3I (5.2 g, 36.6 mmol, 2.63 eq ) were added. The reaction mi ture w as stirred at 25°C for 1 2 hr.. The reaction mi ture was poured into water ( 100 ml. ) and was extracted with EtOAc ( 1 50 mL ). The organic layer was washed by water (80 mL x 2 ), brine (800 mL ) and dried over anhydrous Na2SC<4. The solvent was removed under reduced pressure to give intermediate 442 (2.6 g, 96percent yield ) as a white solid.
Reference: [1] Patent: WO2017/32840, 2017, A1, . Location in patent: Page/Page column 224; 225
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