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Chemical Structure| 4041-21-8 Chemical Structure| 4041-21-8

Structure of 4041-21-8

Chemical Structure| 4041-21-8

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Product Details of [ 4041-21-8 ]

CAS No. :4041-21-8
Formula : C18H21N
M.W : 251.37
SMILES Code : CCCCCCN1C2=C(C3=C1C=CC=C3)C=CC=C2
MDL No. :MFCD08532352

Safety of [ 4041-21-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H341
Precautionary Statements:P501-P202-P201-P280-P308+P313-P405

Application In Synthesis of [ 4041-21-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4041-21-8 ]

[ 4041-21-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 4041-21-8 ]
  • [ 110677-45-7 ]
  • 9-{4-[bis(9-hexylcarbazol-3-yl)methyl]phenyl}carbazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
30% With hydrogenchloride; acetic acid; In water; for 3h;Reflux; 9-hexylcarbazole (1.2 g, 4.6 mmol) hydrochloric acid (10 ml, 35 %) was slowly added to an acetic acid (16 ml) solution of <strong>[110677-45-7]4-(9-carbazolyl)benzaldehyde</strong> (0.5 g, 1.85 mmol) under stirring and the mixture was refluxed for 3 h. The resulting solution was poured into H2O and filtered. The deposit was dissolved in methylene chloride and washed with H2O three times. The separated organic layer was dried over anhydrous Na2SO4. The crude product was purified by silica gel column chromatography using a mixture of ethyl acetate and hexane (vol. ratio 1:25) as an eluent, yielding 0.23 g. (30 %) of a white amorphous solid. 1H NMR spectrum (400 MHz, CDCl3, δ, ppm): 8.13 (d, 2H, J = 8.0 Hz, Ar); 8.02 (d, 2H, J = 7.6 Hz, Ar); 7.96 (s, 2H, Ar); 7.51 -7.36 (m, 16H, Ar); 7.27 (t, 2H, J = 7.4 Hz, Ar); 7.17 (t, 2H, J = 7.4 Hz, Ar); 6.09 (s, 1H, CH); 4.29 (t, 4H, J = 7.4 Hz, NCH2); 1.91-1.84 (m, 4H, NCH2CH2); 1.44-1.37 (m, 4H, NCH2CH2CH2); 1.36-1.24 (m, 8H, CH2CH2CH3); 0.86 (t, 6H, J = 7.0 Hz, CH3). 13C NMR spectrum (400 MHz, CDCl3, δ, ppm): 14.1 (CH3(2C)), 22.5 (CH2CH3(2C)), 27.1 (CH2CH2CH3(2C)), 29.1 (CH2CH2 CH2CH3(2C)), 31.6 (CH2CH2N(2C)), 43.3 (CH2N(2C)), 56.7 (CH); 108.7 (2C); 108.8 (2C); 110.0 (2C), 118,7 (2C), 119.9 (2C), 120.3 (2C), 120.5 (2C), 121.2 (2C), 122.7 (2C), 122.8 (2C), 123.4 (2C), 125.7 (2C), 125.9 (2C), 126.8 (2C), 127.6 (2C), 131.0 (2C), 134.0 (2C), 135.6 (C), 139.7 (2C), 140.2 (2C), 141.0 (2C), 145.0 (C). Elemental analysis for C55H53N3 % Calc.: C 87.38, H 7.07, N 5.56; % Found: C 87.36, H 7.11, N 5.54. IR (KBr, cm-1): 3048 (C-H, Ar); 2953, 2926, 2853 (C-H); 1626, 1598 (C=C Ar); 1483, 1479, 1467 (C=C, Ar and C-H); 1348, 1332, 1316 (C-N, Ar); 1230 (C-N); 798, 770, 747, 724, 627 (C-H Ar).
 

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