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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 40532-06-7 Chemical Structure| 40532-06-7

Structure of 40532-06-7

Chemical Structure| 40532-06-7

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Product Details of [ 40532-06-7 ]

CAS No. :40532-06-7
Formula : C9H9NO2S
M.W : 195.24
SMILES Code : COC1=CC=C(OC)C(N=C=S)=C1
MDL No. :MFCD00041059

Safety of [ 40532-06-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H315-H317-H319-H330-H334-H335-H351-H412
Precautionary Statements:P201-P202-P260-P264-P271-P272-P273-P280-P284-P302+P352-P304+P340+P310-P305+P351+P338-P308+P313-P333+P313-P337+P313-P403+P233-P405-P501
Class:6.1
UN#:2811
Packing Group:

Application In Synthesis of [ 40532-06-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 40532-06-7 ]

[ 40532-06-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 25475-67-6 ]
  • [ 40532-06-7 ]
  • N-(3H-[1,2,4]thiadiazolo[4,3-b]isoquinolin-3-ylidene)-2,5-dimethoxyaniline [ No CAS ]
YieldReaction ConditionsOperation in experiment
96% With montmorillonite K10 Clay; In acetonitrile; at 20℃; for 1h; General procedure: A round bottom flask containing commercially available montmorillonite K10 (10 molpercent) was placed in an oven at 120-130°C for 30 minutes and then it was cooled to room temperature under nitrogen protection. To the activated montmorillonite K10 was added isothiocyanate (3.4 mmol) and <strong>[25475-67-6]3-aminoisoquinoline</strong> (3.4 mmol) followed by acetonitrile (2 mL) at room temperature. The resulting suspension was stirred at room temperature for 1-3 hour. When the reaction was completed (detected by TLC), ethyl acetate (30 mL) was added and the catalyst was filtered off to recover. The organic layer was washed with water (3×30 mL), and finally with half saturated brine, dried over anhydrous Na2SO4 and concentrated by rotary evaporator. Finally, the residue was purified by recrystallization from ethanol.
 

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