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Chemical Structure| 40680-63-5 Chemical Structure| 40680-63-5

Structure of 40680-63-5

Chemical Structure| 40680-63-5

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Product Details of [ 40680-63-5 ]

CAS No. :40680-63-5
Formula : C9H9NO4
M.W : 195.17
SMILES Code : O=C(C1=C(N)C=C(OCO2)C2=C1)OC
MDL No. :MFCD00835593

Safety of [ 40680-63-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 40680-63-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 40680-63-5 ]

[ 40680-63-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 40680-63-5 ]
  • [ 20332-16-5 ]
YieldReaction ConditionsOperation in experiment
65% With water; sodium hydroxide; at 90℃; for 2h; the NaOH (2.95g, 73 . 8mmol) adding water (75 ml) in, stirring to dissolve into the 6 - amino and [d] [1, 3] dioxane -5 - carboxylic acid methyl ester (12.0g, 61 . 5mmol), raising the temperature to 90 C stirring 2 hours. The ice water cooling, concentrated hydrochloric acid to adjust the pH to 2, solids are separated out, full mixing, filtering, the filter cake of water washing, drying shall be 6 - amino and [d] [1, 3] dioxane -5 - formic acid (7.2g, 65%).
 

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