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Chemical Structure| 40899-99-8 Chemical Structure| 40899-99-8

Structure of 40899-99-8

Chemical Structure| 40899-99-8

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Product Details of [ 40899-99-8 ]

CAS No. :40899-99-8
Formula : C16H12N2
M.W : 232.28
SMILES Code : C(N1)(C(N2)=CC3=C2C=CC=C3)=CC4=C1C=CC=C4
MDL No. :MFCD09839789
InChI Key :FFBLFXFOMFDJLS-UHFFFAOYSA-N
Pubchem ID :11020756

Safety of [ 40899-99-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 40899-99-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 40899-99-8 ]

[ 40899-99-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 40899-99-8 ]
  • [ 3616-56-6 ]
  • [ 60511-85-5 ]
YieldReaction ConditionsOperation in experiment
62% With acetic acid; at 100℃; for 1h; General procedure: Dimethylaminoacetaldehyde diethyl acetal (5 mmol) was added to a solution of 7 (0.5 mmol) in AcOH (5mL) at room temperature, and the mixture was heated at 100 °C. After 1 h, the mixture was gradually cooled to room temperature. The mixture was diluted with AcOEt (100 mL), washed with saturated NaHCO3 solution and brine, and dried over MgSO4. The solvent was removed, and the residue was separated by silica gel column chromatography with hexane/AcOEt (5:1) to give 3, 4 and 8.
 

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