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Chemical Structure| 41052-88-4 Chemical Structure| 41052-88-4

Structure of 41052-88-4

Chemical Structure| 41052-88-4

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Product Details of [ 41052-88-4 ]

CAS No. :41052-88-4
Formula : C10H10O2
M.W : 162.19
SMILES Code : O=CC1=CC=C(O)C(CC=C)=C1
MDL No. :MFCD06290488

Safety of [ 41052-88-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 41052-88-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41052-88-4 ]

[ 41052-88-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 28090-12-2 ]
  • [ 41052-88-4 ]
YieldReaction ConditionsOperation in experiment
65% With N,N-diethylaniline; at 190℃; for 20h; The solution of 4-[(3-methylbut-2-en-1-yl)oxy]-benzaldehyde (4.0g, 24.6mmol) in N,N-diethylaniline (20mL) was heated at 190C for 20h. After cooling to room temperature, the mixture was diluted with H2O (20mL) and 6N-HCl (10mL) was added slowly then extracted with EtOAC. The combined organic layers were washed with brine (50mL) and dried over anhydrous MgSO4, filtered, and concentrated under reduced pressure. The residue was further purified by chromatography on silica gel to give 3-allyl-4-hydroxybenzaldehyde (11, 2.50g) as white solid with 65% yield.
 

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