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Chemical Structure| 412341-84-5 Chemical Structure| 412341-84-5

Structure of 412341-84-5

Chemical Structure| 412341-84-5

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Product Details of [ 412341-84-5 ]

CAS No. :412341-84-5
Formula : C9H6N2O4
M.W : 206.15
SMILES Code : O=C1C2=C([N+]([O-])=O)C=CC=C2N=C(C)O1
MDL No. :MFCD27950554

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Application In Synthesis of [ 412341-84-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 412341-84-5 ]

[ 412341-84-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 412341-84-5 ]
  • [ 7732-18-5 ]
  • [ 73721-78-5 ]
  • 2
  • [ 412341-84-5 ]
  • [ 73721-78-5 ]
  • 3
  • [ 412341-84-5 ]
  • [ 64-19-7 ]
  • [ 73721-78-5 ]
YieldReaction ConditionsOperation in experiment
for 2191.5h; Acetic anhydride was selected as an acylation and dehydration reagent. Initially, compound 1 was refluxed in neat acetic anhydride (4.8 equivalents), followed by cooling and filtration to provide compound 2, which contained 5 wt % of acetic acid and was converted to an acetylated compound 1 ,2-acetamido-6-nitrobenzoic acid 1 a, over a three month period under ambient storage in a glass bottle. In order to improve the stability of compound 2, the amount of acetic anhydride was reduced to 2.2 equivalents and isopropyl acetate was used as an alternative solvent.
 

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