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Chemical Structure| 41337-81-9 Chemical Structure| 41337-81-9

Structure of 41337-81-9

Chemical Structure| 41337-81-9

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Product Details of [ 41337-81-9 ]

CAS No. :41337-81-9
Formula : C9H11NO3
M.W : 181.19
SMILES Code : O=C(OCC)C1=NC(CO)=CC=C1
MDL No. :MFCD09750009
InChI Key :CDFOARSBQKJGNL-UHFFFAOYSA-N
Pubchem ID :10921141

Safety of [ 41337-81-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 41337-81-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41337-81-9 ]

[ 41337-81-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 41337-81-9 ]
  • [ 1197-10-0 ]
YieldReaction ConditionsOperation in experiment
89% 6-Hydroxymethyl-pyridine-2-carboxylic acid ethylester (200 mg, 1.1 mmol) (J. Amer. Chem. Soc, 1982, 104,2251-2257) was dissolved in methanol (1 ml). Thereafter, therein 2N NAOH aqueous solution (1 ml) was slowly added dropwise, and the reaction mixture was stirred at room temperature for 1 hour. The reaction mixture was acidified (pH=3) with 2N HC1. Solvent was concentrated under reduced pressure, then, dissolved in methanol and filtered. The filtrate was concentrated under reduced pressure to give 150 mg (yield: 89percent, white solid) of the target compound. 1H NMR (400MHZ, CD30D) : 55. 05 (s, 2H), 8.34 (d, J=8. OHZ, 1H), 8.47 (d, J=8. OHZ, 1H) 8.73 (d, J=8. OHz, 1H)
  • 2
  • [ 1197-10-0 ]
  • [ 20077-29-6 ]
  • [ 39640-51-2 ]
  • [ 41337-81-9 ]
  • [ 287925-06-8 ]
  • 3
  • [ 41337-81-9 ]
  • [ 76292-67-6 ]
 

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