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Chemical Structure| 41727-45-1 Chemical Structure| 41727-45-1

Structure of 41727-45-1

Chemical Structure| 41727-45-1

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Product Details of [ 41727-45-1 ]

CAS No. :41727-45-1
Formula : C10H8Cl2O3
M.W : 247.08
SMILES Code : O=C(O)C1=CC(Cl)=C(OCC=C)C(Cl)=C1
MDL No. :MFCD01660141

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41727-45-1 ]

[ 41727-45-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3336-41-2 ]
  • [ 106-95-6 ]
  • [ 41727-45-1 ]
YieldReaction ConditionsOperation in experiment
92% (a) Synthesis of a Selector of the Cation-Exchange Type For a synthesis of 4-allyloxy-3-5-dichlorobenzoic acid chloride, 9.7 mmol <strong>[3336-41-2]3,5-dichloro-4-hydroxybenzoic acid</strong> (Acros Organics, Geel, Belgium), 20 mmol potassium hydroxide and 11.6 mmol allyl bromide (Aldrich) were refluxed in ethanol for 24 hours. Upon the hydrolysis of ester by-products with 1.8 M of a potassium hydroxide solution, the carboxylic acid was precipitated by acidification with 2M HCl. Recrystallization from petroleum ether-methanol produced the pure carboxylic acid at a yield of 92percent.
 

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