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Chemical Structure| 42936-88-9 Chemical Structure| 42936-88-9

Structure of 42936-88-9

Chemical Structure| 42936-88-9

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Product Details of [ 42936-88-9 ]

CAS No. :42936-88-9
Formula : C11H13ClO3
M.W : 228.67
SMILES Code : CC(C)(OC1=CC=C(Cl)C=C1C)C(O)=O

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Application In Synthesis of [ 42936-88-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 42936-88-9 ]

[ 42936-88-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 42936-88-9 ]
  • [ 62058-03-1 ]
  • C21H28ClNO3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Example B.I Preparation of compound 1; 1 -Hydroxy- lH-benzotriazo Ie (0.0007 mol) was added to a solution of intermediate 1 (0.0006 mol) in dichloromethane (10 ml) and DMF (5 ml) and the mixture was stirred for 10 minutes. Then JV"-(ethylcarbonimidoyl)-iV,iV-dimethyl- 1,3-propanediamine, monohydrochloride [25952-53-8] (0.0007 mol) was added and the mixture was stirred for 20 minutes. After addition of (lalpha,3alpha,4alpha,5beta,7alpha)- 4-aminotricyclo[3.3.1.13'7]decan-l-ol [62058-03-1] (0.0007 mol), the reaction mixture was stirred overnight and the solvent was evaporated. The obtained residue was dissolved in dichloromethane and then washed with a 15 percent citric acid solution and with a Na2CO3 solution. The organic layer was dried through Extrelut and the solvent was evaporated, yielding 0.17O g of compound 1.
 

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